Chemistry 334: Organic Chemistry Majors Laboratory II

Spring 2014, University of Delaware

 

 

Laboratory Coordinator:          Dr. Geoffrey Sametz

sametz@udel.edu (questions about the lab should be directed here or to your TA)

 

Teaching Assistants:                William Reid    Section 11       MTu, 7:00-10:00p, QDH318

Peng Wang      Section 12       MTu, 3:45-6:45p, QDH318

Jennifer Eddy  Section 13       WTh, 12:30-3:30p, QDH318

                        

 

Syllabus (updated 2/17)

Example Notebook Entry

 

 

Schedule of Experiments (updated 3/3)


Week (Dates)

Lab/Handout

1 (2/10 – 2/14)

No Lab

2 (2/17 – 2/21)

Safety (Right to Know)

3 (2/24 – 2/28)

Determination of Unknown using Spectroscopy

4 first lab session

canceled due to weather

4 second lab session

Ketone Reduction with Carrots

5 first lab session

Ketone Reduction with Carrots con't

5 second lab session

Oxidation of Borneol

6 first lab session

Oxidation of Borneol con't

6 second lab session

Heck Coupling

7 first lab session

Heck Con't/ Suzuki Coupling

7 second lab session

Suzuki Coupling

(3/31 – 4/04)

Spring Break

8 (4/07 – 4/11)

Aldol Condenstaion/Transfer Hydrogenation

9 (4/14 – 4/18)

Reductive Amination

10 (4/21 – 4/25)

Biodiesel

11 (4/28 – 5/02)

Coumarin Synthesis

12 (5/05 – 5/09)

Laboratory Practical

13 (5/12 – 5/16)

Laboratory Practical

TBA

Final Exam

 

 

Lab Technique Handouts

Recrystallization

Preparation of NMR samples

Operation of IR100 Spectrometer

Using M-Nova

 

Additional Safety Links and Documents

UD Environmental Health and Safety (EHS)

EHS Chemical Hygiene Plan

EHS Hazardous Materials Saftey Manual